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GCMS analysis results for sample AD26676, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26676 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031968–000031988

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000031982
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26676. D Vial: 9 Acq On 6 Dec 2001 5:28 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 3-Hexanol Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

6.70 0.4.5 ng/uL 138267 1,4-Dichlorobenzene-d4 11.89

Hit# of Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3 -Hexanol 102 C6H140 000623-37-0 64 4 3-Hexanol 102 C6H140 ______ 000623-37-0 64 Abundance Scan 203 (6.701 min): 26676.D (-) m/z 59.10 100.00%| I 59 55 I I | 5000 73 43 TIP -A0 ; 39 6.40 6.60 6.80 7.00 ! ......................... Ill H 11111 1 ।1 1 —+ — ■ i ■ • ■ ■ । ■ • ■ ■ । ■ i ■ m/ z 55.05 71.11% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63528: 3-Hexanol 59 55

5000 73 A— A4PP—4 -PR- 31 6.40 6.60 6.80 7.00

27 m/z 73.05 41.18% 1 45 84 TI-TTTTTTTrUr TTTT । I | ,-n-i-p-r — TTTT TTrrTr i , । ।, m/z-s 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ■Abundance #63531: 3-Hexanol 59 55 ------------ A- I > । । । । । । Z । 6.40 6.60 6.80 7.00 5000- 73 m/z 43.05 24.15% 43 39 69u—TEuuuntir • | ■ ■ " ■ | ■ • • ■ | • • ■ • | » I • rn-pTi’i TT 1—1.21. ‘‘‘‘0‘1‘t1——‘ . ,,,,,, m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63527: 3-Hexanol ' ' ■ i 1 ■ ' ' i ■ 1 ■ 1 i ' 1 1 1 I1 1 ’ 1 1

55 5 6.40 6.60 6.80 7.00

(OOJ m/z 41.05 23.41% 5000 73 31

27 45 - I S j m TPPE PPP 4+4 H 84 11 ■' ■ ■ । ■ ■ ■ ■ । •' • ■ । " m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 6.40 6.60 6.80 7.00_____

26676.D NP112701.M Fri Dec 07 14:51:34 2001 Page 7

NYC-WTC_000031982

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NYC-WTC_000031982Source: NYC Law Department, mirrored locally

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