GCMS analysis results for sample AD26678, Dec 10 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26678.D Vial: 4 Acq On 4 Dec 2001 1:33 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 3-Hexanol Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

6.66 0.43 ng/uL 117813 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 74 3 3-Hexanol 102 C6H140 000623-37-0 74 4 3-Hexanol 102 C6H140 000623-37-0 74 Abundance Scan 199 (6.664 min): 26678.D (-) m/z 59.10 100.00% 55 59

5000 73

41 — --A 6.40 6.60 6.80 7.00

m/z-> +++. +ir I""... I I" •' 11' ‘ * I • •' • I *' " I “ •' p ' " I T‘ m/z I'"*i"'’I"‘’I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 55.10 89.59% Abundance #63529:3-Hexanol 59 55

5000 31 73 27 6.40 6.60 6.80 7.00 m/z 73.05 47.02% 44 | , mll I.. ""I 102 i ■ " 'i'' ” r " ' i■ " • i" " i" i ■ miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1 762; 3-Hexanol 59 55 31 6.40 6.60 6.80 7.00

WNA 5000- 27 43 73 m/z 41.05 18.04%

102 ‘TTTT _______________ !_______________ i' ■______________ ,iii._____________ 1‘00‘1000‘1111000UNM1"TT I ",l l " 1111"' i ■" ■ i" " i" " i " ■' I" । ■ i" ‘ ■ i" " i miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63528: 3-Hexanol 55 59 6.40 6.60 6.80 7.00 m/z 39.10 11.72%

MMW 73 5000 31

| m/z-> m 27 P ।. P .. i45PToor 84 IP 1WTITTTTT +4 p r. < । n r. p . ., J 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 T‘ 6.40 6.60 6.80 7.00 |

26678.D NP112701.M Fri Dec 07 13:08:45 2001 Page 6

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