GCMS analysis results for sample AD26680, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26680.D Vial: 3 Acq On 4 Dec 2001 12:38 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 3-Hexanol Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

6.69 0.47 ng/uL 126690 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 78 4 3- Hexanol 102 C6H140 000623-37-0 74 Abundance Scan 201 (6.688 min): 26680.D (-) m/ z 59.10 100.00% 55 59

5000- 73 41 .... ....................................... .. 6.40 6.60 6.80 7.00 pf.. । । -HP— +4 I ' " ' I i ■ ■" i • • ■ ■ i" • ■ i " ■ ■ r "' i" " r " • i ■ m/z 55.10 76.32% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529: 3-Hexanol 59 55

5000 31 ) - 73 27 6.40 6.60 6.80 7.00 m/z 73.05 39.41% I 44 ' , 1" 1 'I —I m mH 1..... TTCTTTTT’T’T >... 1.... j.... 1. 102 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 10G 105 110 Abundance #53527:3-Hexanol 59 I 55 6.40 6.60 6.80 7.00 5000 73 m/z 41.05 27.42% 31

m/z-> Abundance 27 TTp ■ i" • ■ i • i'. i1 •1 • I 45 84 T’’01—1001IWVIBITTT TTTTTTTTTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #63531: 3-Hexanol v W UNA 1 ' ' I 1. I I I I I I . II . I TT I

55 59 m/z 6.40 6.60 6.80 7.00 43.05 22.39% 5000- 73

43

TrHtm TTTT +4 -69 39 V |i>>>j.r>«।■ r.■। 111 I " '' r " ■ r ■'' r ■ " i' ■ ' i ' ' ' '"I ' 1 ' 1 I TTTT । m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00

26680.D NP112701.M Fri Dec 07 13:11:40 2001 Page 8

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