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GCMS analysis results for sample AD26680, Dec 10 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26680 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032058–000032078

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC04 0l\26680.D Vial: 3 Acq On 4 Dec 2001 12:38 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 2-Hexanone Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

6.55 0.51 ng/uL 136242 1,4-Dichlorobenzene-d4 11.87

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 90 2 2-Hexanone 100 C6H120 000591-78-6 90 3 2-Hexanone 100 C6H120 000591-78-6 90 4 2-M exanone, 4-hydroxy-3-propyl- 158 C9H1802 _______ 062338-17-4 74 'Abundance Scan 186 (6.551 min): 26680.D (-) m/z 43.00 100.00% 43

5000-

391 —H — 4 nmmmpmmmmmpm m/z 58

71 85 100 QJ 6.20 6.40 58.10 6.60 6.80 54.98% 7.00 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63385: 2-Hexanone 43

-------- 5000- 58 6.20 6.40 6.60 6.80 7.00 29 m/z 57.05 16.56% 39 71 85 100 — ......... 1.......... IDpi I T — I • • • ‘ I rrp-r 111111 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 [Abundance #1556: 2-Hexanone 43

6.20 6.40 6.60 6.80 7.00 58 5000- m/z 41.10 13.76%

27 39 71 85 100 i l ■ ■ i T‘ i"" i ■ ‘"I "■■ r ■ " i''■ I"f'i' >" i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 'Abundance #63384: 2-Hexanone 43 6.20 6.40 6.60 6.80 7.00 m/ z 39.00 8.19% 5000- 58 29

miz-> 39 - " 1" -H+ TTTTTTmmTTTT | 71 85 T" ‘ ’ l 100 I_____________ " I'1' • I' " ‘ I 2 AA MAA A 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80 7.00

26680.D NP112701.M Fri Dec 07 13:11:38 2001 Page 7

NYC-WTC_000032071

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