GCMS analysis results for sample AD26828, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26828.D Vial: 12 Acq On 6 Dec 2001 8:12 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 3-Hexanone Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

6.46 0.50 ng/uL 124390 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 90 2 3 -Hexanone 100 C6H120 000589-38-8 90 3 3-Hexanone 100 C6H120 000589-38-8 78 4 3-Hexanone 100 C6H120 _________ 000589-38-8 4 0 Abundance / Scan 177 (6.462 min): 26828.D (-) m/z 43.10 100.00%

GL 43 57 71 5000 100 39

miz-> T’T 4 ............ H 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 T’TTTTTTTTT •Hr । WINIWHgTT I‘ I m/z 6.20 6.40 57.10 6.60 6.80 92.84% Abundance #63358: 3-Hexanone i 43 I 57 I i 71 5000- 6.20 6.40 6.60 6.80 100 m/z 71.05 55.48% I 85 T’TTT 11. >. P I • 11 TT i । ■ ■ ■ ■ । 11 rqm i pi. rrp i i i | 1' i1" ‘ i'11111 1'"' I I" •' I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 'Abundance #1528: 3-Hexanone I 43 57 TI—T -------- ' ri 11 1-1 1 6.20 6.40 6.60 6.80 29 71 5000- m/z 100.15 29.70% 100 85 I " " 11''' I TT T TT TTTTTTTTTTTTT l■ ■ ■ ■l • • ■ ■ I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357:3-Hexanone 43 6.20 6.40 6.60 6.80 57 29 m/ 41.00 27.67% 5000- 71

100

miz- mp— i I " ‘' I ‘ ” 111 ‘ 1 r " ' r " ' i1 ‘' i" " r " ■ i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 +.. 85.. " i " ■ • i 6.20 6.40 6.60 6.80

26828.D NP112701.M Fri Dec 07 14:53:25 2001 Page 5

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