GCMS analysis results for sample AD26680, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26680.D Vial: 3 Acq On 4 Dec 2001 12:38 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 3-Hexanone Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

6.45 0.45 ng/uL 121820 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 90 2 3-Hexanone 100 C6H120 000589-38-8 83 3 Buta: , 2,2-dimethyl- 86 C6H14 000075-83-2 59 4 3-He' anone 100 C6H120 000589-38-8 43 Abundance ‘ Scan 175 (6.450 min): 26680.D (-) m/z 43.05 100.00% 43 57

71 5000- 100

m/z-> 5 TTTTTIT’TT l ,85TTTTTt 10 15 20 25 30 35 40 45 50 55 60 65 70 75 BQ 85 90 95 100105 1" r " ■ i" " r'" r "' i I" "I 6.00 6.20 6.40 6.60 6.80 m/z 57.00 83.36% Abundance #63358: 3-Hexanone I 43 57 i 5000 71 —1 6.00 6.20 6.40 6.60 6.80 100 m/z 71.05 55.58% 85 r ■ "i" r ■" i +TTTTT '' I" " I'" ’ I +rr TTT m/z- 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1528: 3-Hexanone 43 57 TT—mmT

5000 29 71

100 m/z I, 6.00 6.20 6.40 6.60 6.80 34.63%

85 I" " r"' r ■ "i" " r" 'i" " i' ■ "i i"”TUpTr'i"111"''I""i'r "’i'"11""I m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ‘Abundance #732: Butane, 2,2-dimethyl- 43 57 6.00 6.20 6.40 6.60 6.80 I 71 m/ 41.00 18.49% 29 5000

15

'''' i'''' I'''' i' ‘‘ i' T1 n 'T1" 11 h........... I Tprrrrp-rrr *——""——811 m/z-> 5 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80

26680.D NP112701.M Fri Dec 07 13:11:36 2001 Page 6

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