GCMS analysis results for sample AD26679, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 4 01\26679.D Vial: 5 Acq On 4 Dec 2001 2:27 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 6 3-Hexanone Concentration Rank 19

R.T. EstConc Area Relative to ISTD R.T.

6.47 0.47 ng/uL 159595 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 86 2 3-Hexanone 100 C6H120 000589-38-8 83 3 3-Hexanone 100 C6H120 000589-38-8 78 4 3-Pentanone, 2-methyl- 100 C6H120 000565-69-5 50 Abundance Scan 178 (6.472 min): 26679.D (-) m/z 43.10 100.00%

N 43 57

5000- 71 100 39 6.20 6.40 6.60 6.80 I m/z-> TTTTTTTTTT — 53 TPPTTI 20 25 30 35 40 45 50 55 60 +85 r ■ ■ 'i 65 70 75 80 85 90 95 100 105 m/z 57.05 89.47% Abundance #63358: 3-Hexanone 43 57

5000 71

100 AAA 6.20 6.40 6.60 6.80 f

m/z 71.05 48.91%

m/z-> i ’ *'11 tr HT II "r"■i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 + Abundance #63357:3-Hexanone 43 29 57 --------A---------- 6.20 6.40 6.60 6.80 5000 71 m/z 100.15 31.73% 100 i i 85 T*BOO— 0—00UUUTTTCTTTTTTTTT""T"T"ITTTT p-TTT "I''"I m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 43 #63356: 3-Hexanone MA A 29 57 6.20 6.40 6.60 6.80

1 m/z 41.05 22.11% 5000 71

100

m/z—> 1' i" " i' 3,4 TTTTTTTTTT TTTTTTTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ....... 85........ " 11'" I 6.20 6.40 6.60 6.80

26679.D NP112701.M Fri Dec 07 13:10:11 2001 Page 6

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