GCMS results log, sample AD26985, Dec 11 2001

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Library Search Compound Report

Data File C: \HPCHEM\1\DATA\DEC0601\26986. D Vial: 32 Acq On 7 Dec 2001 3:19 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P .

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 7 3-Hexanol Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

10.32 0.78 ng/uL 308880 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol/ 102 C6H140 000623-37-0 40 2 3-Hexanol 102 C6H140 000623-37-0 38 3 3-Hexanol 102 C6H140 000623-37-0 38 4 3-Pentanol, 2-methyl- 102 C6H140 000565-67-3 25 Abundance Scani 598 (10.322 min): 26986.D (-) m/ z 43.10 100.00% 43

55 59 5000 73 85 TEir —A—, — m/z-> I ’ " ‘ I" •' I 4 4 - H+ 39

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 100 1WBI]PPum*aUugr m/z 10.00 10.20 10.40 10.60 59.10 55.00% Abundance I #1762: 3-Hexanol 59 55

5000- 27 31 43 73 s 10.00 10.20 10.40 10.60 m/z 55.10 50.40% l iH . ] rrt i j rrri ] tH i | 102 I ” " I •' ‘' I 11 ’' 11111 I.............. T" 111 T T m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63527:3-Hexanol : 5553 -A 10.00 10.20 10.40 10.60 5000- 31 73 m/z 57.10 35.03%

27 45 ,‛i 84 —TUTp TIT i''" i" " I' ■ " r ■" i " " i •'" r "' i" ■11 " ' ■ r ' TTTTT '11"'11' miz-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #63529: 3-Hexanol AAA 55 59 ___ 10.00 m/z 50.20 41.10 10.40 10.60 32.39% 31 5000 73 27 / l'

m/z-> TTTTTTTTT Trr m -H 4+ — 44 102 "TCTTTTTTTTTTTT I ■ 1 ■ | 1 ■ . t | . I I | I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 1 ' । 1 — —4 10.00 10.20 10.40 10.60

26986.D NP112701.M Tue Dec 11 14:51:31 2001 Page 7

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