GCMS analysis results for sample AD26679, Dec 10 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC04 01\26679.D Vial: 5 Acq On 4 Dec 2001 2:27 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 3-Hexanol Concentration Rank 20

R.T. EstConc Area Relative to ISTD R.T.

6.70 0.44 ng/uL 149870 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hex, ol 102 C6H140 000623-37-0 83 2 3-P ntanol 88 C5H120 000584-02-1 64 3 3 Hexanol 102 C6H140 000623-37-0 64 4- 3- Hexanol 102 C6H140 000623-37-0 64 Abundance Scan 203 (6.701 min): 26679.D (-) m/z 59.10 100.00% 59

5000 73 43 —fr $47.00 —S 6.40 6.60 6.80 - - - ---+ th——- —— ■ ' i 1 • ■ • i ■ ■ ■ ■ i ■ ■ > ' i ■ ■ ■ • i m/z 55.10 76.86% m/z->______ 10 20 30 40 50 60 70 80 90 100 110 Abundance #63531: 3-Hexanol 59

5000 73 1 4 . , --A-PR-1 6.40 6.60 6.80 7.00 43 m/z 73.05 44.18% 1IIf H.... TIl, ।.____ i i . . 1 . _______________ . . , । . . . . । , ! m/z->10 20 30 40 50 60 7C 80 90 100 110 Abundance #851: 3-Pentanol 59 1 31 6.40 6.60 6.80 7.00 5000 m/z 43.05 31.83% 41 15 26 1 ' ■ i ' 1 ' 1 i ■ ■ i 1d1t**11/--01——-1/1//*—T1**11B.T। । ' । । < । । i~ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1762: 3-Hexanol ' —P ----- 59 6.40 6.60 6.80 7.00 m/ z 41.00 23.35% 31

miz-> 5000 -

— T ------- । । ——— Ji 10 2G 30 40 43

50 60 73

90 102 Ir ' ' i 1 ■ ■ ' r ■ • ' ' i ' ' ’ ' TT1nn 70 80 | 100 110 6.40 AAW W— — 6.60 6.80 7.00

26679.D NP112701.M Fri Dec 07 13:10:15 2001 Page 8

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