GCMS results log, sample AD26985, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26986.D Vial: 32 Acq On 7 Dec 2001 3:19 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 2-Hexanol Concentration Rank 17

R.T. EstConc Area Relative to ISTD R.T.

10.52 0.45 ng/uL 177546 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexane 102 C6H140 000626-93-7 45 2 2-Hexanol 102 C6H140 000626-93-7 45 3 2-Pentanol, 3-chloro-4-methyl-, (R@ 136 C6H13C1O 074685-47-5 39 4 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 39 Abundance Scan 620 (10.524 min): 26986.0 (-) Hm/ z 45.10 100.00% i 45

5000 41 TT—mBB/n/T 57 60 85 10.20 10.40 10.60 10.80

m TT wl5... 1......... 1..... —00. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/ Z 43.10 88.29% Abundance #63583: 2-Hexanol 45

5000 - II L 10.20 10.40 10.60 10.80 m/z 41.10 32.80% 27 — 69।

m/z-> ■11 ■" ■ । ■ -31--— 55 87 Trir 111111111111111111111111

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1792: 2-Hexanol 45 ----- —P 4 10.20 10.40 10.60 10.80 5000 m/z 57.10 17.36%

27 55 69 31 39 , 87 TIT TTTTT _A A ' ■ i' ■'' i ■ r ' " i ■" ' i' ■ ■' r'" i' " ' i " " i ■ •" i ■ ’" i" ■ ■ r ■" i " •' i " " i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #6421: 2-Pentanol, 3-chloro-4-methyl-, (R@,R@)-(.+/-.)- 45 10.20 10.40 10.60 10.80 m/ Z 44.00 15.95% 5000

27 58 69 76 85 100 —mmmTTTTTT T-p-r TI]WHU——eUT i1"' i ' ' I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 10.20 10.40 10.60 10.80

26986.D NP112701.M Tue Dec 11 14:51:33 2001 Page 8

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