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GCMS analysis results, sample AD27547, December 2001

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of environmental sample AD27547 performed on 12/18/01, detecting unknown compounds with 2,4-DDD surrogate standard at 5.0 ug MDL.

NYC-WTC_000033458–000033473

Folder label: “GCMS X 11/15/01 A 12/13/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\DEC1301\27547.D Vial: 6 Acq On 13 Dec 2001 2:56 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

6.81 0.41 ng/uL 153054 1,4-Dichlorobenzene-d4 11.87

Hit# Of 5 entative ID MW MolForm CAS# Qual

l 2-Hexanol/ 102 C6H140 000626-93-7 74 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 64 3 2-Pentanol , 4-methyl- 102 C6H140 000108-11-2 64 4 2-Hexanol 102 C6H140 000626-93-7 64 Abundance Scan 214 (6.805 min): 27547.D (-) m/ z 45.10 100.00% 45

5000 -

69 T1 r1 Pr । 56 | 84 6.40 6.60 6.80 7.00 7.20 207 I'1" I T1 rh TTTT .*11111111 i'i 1111111111111111।। > 111। । । ■. >. । r r m/z 69.10 15.13% m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 210 Abundance #63583: 2-Hexanol 45

5000 6.40 6.60 6.80 7.00 7.20 69 m/ z 43.10 14.21% 27 55 __ I I 87 i' Tit i TTTT TUTITT I ‘ ‘IT l”" l"4g l i" " I"'' i " " r ' " I m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 Abundance #63546: 2-Pentanol, 4-methyl- 45

6.40 6.60 6.80 7.00 7.20 5000- m/ z .41.05 12.05% 27 69

, NM. _ 1 57 । 87 m/z-> 10 20 30 40 50 60 70 80 90 100110 120130 140 150 160 170 180 190 200 210 Abundance #63547: 2-Pentanol, 4-methyl- 45 6.40 6.60 6.80 7.00 7.20 "... 8.71% 5000 -

27 69 ......1 Tn r'" r "' i 57 87 TH 1‘ , j.... ।.... 11111111 n-p ।।।। MAAplnt m/z--> 10 20 30 40 50 60 70 80 90 100110 120 130 140150160 170 180190 200 210 6.40 6.60 6.80 7.00 7.20

27547.D NP112701.M Fri Dec 14 12:55:25 2001 Page 3

NYC-WTC_000033468

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NYC-WTC_000033468Source: NYC Law Department, mirrored locally

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