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GCMS analysis results for sample AD28166, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD28166 conducted on January 2, 2002.

NYC-WTC_000034669–000034685

Folder label: “GCMS X 11/23/01 A 12/21/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2101\28165.D Vial: 15 Acq On : 22 Dec 2001 6:40 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.75 0.69 ng/uL 184361 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 2-Hexanol 102 C6H140 000626-93-7 83 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 74 3 2-Hexanol 102 C6H140 000626-93-7 74 4 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 74 AbundanceZ Scan 208 (6.752 min): 28165.D (-) m/z 45.10 100.00% 45

5000

69 6.406.60 6.80 7.00 7.20 _______ i III 55 | 87 pTrrpTTrprn prtTprf rpn r TtttTTT. > I’TT I0‘00—010——00——09—9"“T0—“*"OOBBBu—nur 207 15.52% miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 210 Abundance #63583:2-Hexanol 45

5000 IM-Pr 6.40 6.60 6.80 7.00 7.20 m/z 69.10 14.62% 27 — 69 55 1 87 TTTT । n p 11H tpmmmTDT TTUTTUTTpppT> 111111 m/z-> 10 20 30 40 50 60 70 80 90 100110 120 130 140150160170 180190200 210 Abundance #63546; 2-Pentanol, 4-methyl- 45 6.40 6.60 6.80 7.00 7.20 5000 m/z 43.10 13.42% 27 69 1 57 j 87 i | | I H । H /. । i i i i । m TRTTTTTTT , I , , ■ . . . . . . . ■ , . , . , , . ■ ■ , ■ ■ , . ■ , ...... miz-> 10 20 30 40 50 60 70 80 90 100110120130140 150160 170180 190200 210 - Abundance #1792:2-Hexanol ......................... .. 1 r 11'1 ■ ■ i1 45 6.40 6.60 6.80 7.00 7.20 m/z 44.10 11.63% 5000

miz—> — 27 । i ।. p— ,.JLl.i.... TTTT pTTq-rrrrpn 55 69 87 "‘1111i" 111'1_'' ______________________________________ 1 i. । «... j।. |Tm TWPOOgpuTTT 10 20 30 40 50 60 70 80 90 100 110120 130140150160 170180190200 210 MA6.60 6.80__7.00 7.20 6.40

28165.D NP112701.M Fri Dec 28 09:57:11 2001 Page 4

NYC-WTC_000034680

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NYC-WTC_000034680Source: NYC Law Department, mirrored locally

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