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GCMS analysis results for sample AD27631, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27631 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033177–000033190

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\DEC19 0127631.D Vial: 19 Acq On : 20 Dec 2001 2:19 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.82 1.59 ng/uL 426332 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 entative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 83 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 78 3 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 74 4 2-Hexanol 102 C6H140 000626-93-7 64 Abundance, Scan 215 (6.816 min): 27631.D (-) m/z 45.10 100.00% 45

5000 - 41 69 84 87 6.40 6.60 6.80 7.00 7.20

m/z-> 10 15 20 25 30 35 38 44 ,....... 535,659 1u—n—uumm—ugr m prm m/z 50 55 60 40 4570 80 85 90 95 65 1 75 69.10 13.62% Abundance #63584: 2-Hexanol 45 / s 5000 6.40 6.60 6.80 7.00 7.20 69 m/ Z 41.10 12.12% 19 — 44 27,31 56 | 84 8/ T

NW T TH tTgu....... 11 ■ ■■■■T TTTTTrrr TTT ' 'i TTT (TTT ■' i' m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63547: 2-Pentanol, 4-methyl- 45 Prfmr i I ' ' ' ' I ' ' ' ' I ' ' ' l 6.40 6.60 6.80 7.00 7.20 5000 - m/ z ,43.10 11.94%

27 1 t. 69 57 । 84 87 ......................... •............... 38 i .......... TTT 11 TTTTTTT’TTTT t t I I I t t I I ( t I I I I • I I I ■ I ■ I ■ . 1111111 TTg . 11 • > 11TTT m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546: 2-Pentanol, 4-methyl- 45 6.40 6.60 6.80 7.00 7.20 m/z 44.10 8.47% 5000

27 _ 69

m/z-> 10 19 111'' i'1'1) " ‘1 f111' 11 15 20 25 | 31 -42

30 35 40 57 TIIP—TT TTTTTT I 84 87

45 50 55 60 65 70 75 80 85 90 95 LAAAL. 6.40 6.60 6.80 7.00 7.20

27631.D NP112701.M Fri Dec 21 09:19:56 2001 Page 4

NYC-WTC_000033188

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