GCMS analysis results for sample AD27765, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD27765 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033311–000033342

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\DEC1901\27765.D Vial: 8 .Acq On : 20 Dec 2001 2:18 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 2-Hexanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.79 3.00 ng/uL 673371 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 'entative ID MW MolForm CAS It Qual

1 2-Hexanol/ 102 C6H140 000626-93-7 83 2 2 - Hexanol 102 C6H140 000626-93-7 83 3 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 74 4 2-Pentanol, 4-methyl - 102 C6H140 _________ 000108-11-2 74 Abundance i Scan 213 (6.794 min): 27765.D (-) m/z 45.10 100.00% 45

5000

41 69 IIP 4..... 6.40 6.60 6.80 7.00 7.20

miz-> 38 —4 . ......... ....................... 11... ,r.r 79.4444..... 50 53 56 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 | 72 m/ Z 41.10 14.66% 'Abundance #1792: 2-Hexanol 45

5000 6.40 6.60 6.80 7.00 7.20 m/z 69.10 13.76% 69 27,31 TTTTmuTmgiuti 39 42, ■ i ■ ■ ■ 55 58 ■ 11 > > > ।. 84 87 ■ ■ । । ।1' ■ ■ i > m/z—> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584 ; 2-Hexanol 45 =TTr 6.40 6.60 6.80 7.00 7.20 5000- m/ z 43 . id 11.91%

69 19 27 31 42,. 56 84 87 TTTTTIIT ■ i " r 1 r 11' r 1111 ‘1111111 11 ■ ■ • ■ r 1" 111 ■ ■ i"'' r ■ r ■ ■ ■ i" ■ ■ i'' • ■ i • •' ■ i ■ m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546: 2-Pentanol, 4-methyl- 1 I ' 1 1 1 1 1 ' 45 6.40 6.60 6.80 7.00 7.20 m/ z 44.10 10.90% 5000

27 69 19 | 31 42 57 | 84 87 m/z-> IVuuuug—uutur 10 15 20 25 30 35 m + • i • > • ■ 111 ■ ■ । ■ ■ • ■ । 40 45 50 55 60 65 70 75 80 85 90 95 11 ■ ■ > • । ■ > • ■ । ■ 11 • 1 ■ ■ i ■ • ■ ■ i ■ ■ 6.40 ■ ■ । 6.60 ■ i 11 1 1 TTPTrr 6.80 7.00 7.20

27765.D NP112701.M Thu Dec 20 11:23:42 2001 Page 8

NYC-WTC_000033326

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NYC-WTC_000033326Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AD27679, Jan 2002 · Box DEP Box 21

NYC-WTC_000033263

Laboratory report documenting GCMS analysis of sample AD27679 for unknown compounds and surrogates on January 3, 2002.

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