GCMS unknowns analysis results for sample AD27952, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27952.D Vial: 8 Acq On : 20 Dec 2001 10:32 pm Operator: GALOS Sample : gems unknown 11/20 Inst. : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

6.82 0.77 ng/uL 309282 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Pentative ID MW MolForm CAS# Qual

1 2-Hexanol/ 102 C6H140 000626-93-7 83 2 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 83 3 2-Hexanol 102 C6H14O 000626-93-7 83 4 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 74 Abundance " ’ Scan215 (6.816 mln): 27952.D (-) m/z 45’16 100.00% ! 45

5000

41 69 6.40 6.60 T-r-r 6.80 P ... 7.00 7.20

m/z-> 10 15 20... 25 30 35 +4 ... 53,5659.....4......... ...... — m/ z 40 45 50 55 60 65 70 75 80 85 90 95 69.1,0 14.10 Abundance #63583:2-Hexanol 45

5000 T ■ n , ,0 , TT IT . —IT — 6.40 6.60 6.80 7.00 7.20 . 69 m/z 41.10 12.58 27 31 39 42, 55 58 | i1 ■' ■ i ■1 H 11'111'1'11 ■ ■' i11'11 ■1 ■ ■ 1 r • I»• • ■ 11 < i • i ■ ■ ■ ■ । ■111 •i>। 84 87 । ‘ • 1111 > ■ 111 > 1111 miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #$3547; 2-Pentanol. 4-methyl- 45 11 6.40 6.60 6.80 7.00 7.20 5000 m/ z 43.05 11.52 27 38 A 42 ; , 57 69 84 87 | r ■ ■ >)1 I > * | * r. i ] H 11. k. । > k.. । rt 111 ■ i ■ ■ 111 ■ 11111111111111 ■ 11111 11111 ■ i ■ ■ TIpir TITT TTp m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584: 2-Hexanol PA ' ■ i 1 1 1 ■ i 1 1 1 45 6.40 6.60 6.80 7,00 7.20 m/z 44.10 9.31% 5000

69 TgrTm 1 -AAA. । , -4— - 1 84 87 miz-> -19 . .... . 56 10 15 20 25 30 35 40 45 50 55 60 65 6.40 6.60 6.80 7.00 7.20 70 75 80 85 90 95

27952.D NP112701.M Fri Dec 21 10:05:48 2001 Page 4

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