GCMS unknowns analysis results for sample AD27952, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27952.D Vial: 8 Acq On : 20 Dec 2001 10:32 pm Operator: GALOS Sample : gems unknown 11/20 Inst. : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.71 0.54 ng/uL 219844 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 90 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 000623-37-0 83 Abundance Scan 203 (6.706 mln): 27952.D (-) m/ z 59.1,0 100.00% 55 59

5000 73 43 1 39 -------4-- — .... 6.40 6.60 6.80 7.00 • ■ i • • ■ • i

— — > | >» TT 4# 1 ' ' ' I | M M69I ! !I I ■ | I I ■' i ■ ■ ■84 11 " '11'1 ■' i ■ ■ i ■ ■" r ■ m/z 55.1.0 !90.26% miz-> 20 25 30 35 40 45 50 55 60_ 65 70 75 80_ 85 90 Abundance #63531: 3-Hexanol 59 55

5000 43 73 -A ___ 6.40 6.60 6.80 T 7.00 m/z 73.05 44.03% i 39 4m l ■ ■ l " • ■ • l • • ■ ■ l ■ ■ »• j ■ ■ ' 11 ■ l miz->_____ 20 25__ 30__ 35 40 45 50 55 60 65 fpu i111 ‘ i ■ -8+ ..... 70 75 80 85 90 Abundance #63528: 3-Hexanol i 59 55 \____________ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ । ■ • > > । ■ • > ■ । 6.40 6.60 6.80 7.00 73 5000 m/z 43.10 32.40% 31 27 45 m/z-> ■ • I " '' i1 20 25 11 --- 30 35 40 45 50 55 60 65 70 75 td . 80 85 90 Abundance #63527:3-Hexanol . 59 1 ' 1 i ' 6.40 -A- 6.60 6.80 7.00 55 m/z 41.10 26.97%

m/z-> 5000

27 " I " " 111 " I 20 25 30 31

• i ‘‘ 35 45 ■ i ■ ■ ■ ■ I' ■ ■' i ■ 40 45 50 4m mH 73

84 • i • ■ ■ ■ i ■' < ■ i • ■ ■ ■ i ■ ■ 55 60 65 70 75 80 85 90 _ MuA ___ 6.40 | » I ! | I I , , | I ! , » | I "I I I 6.60 6.80 7.00

27952.D NP112701.M Fri Dec 21 10:05:46 2001 Page 3

NYC-WTC_000034083