GCMS analysis results for sample AD28167, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC2101\28168.D Vial: 18 Acq On : 22 Dec 2001 10:19 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 3-Hexanol Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

6.63 0.41 ng/uL 106182 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 x Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 ____ 000623-37-0 78 Abundance * Scan 195 (6.634 min): 28168.D (-) m/z 59.10 100.00% 55 5

5000 73 43 39 —A6.60A . 6.80 ..6.40 6.20 ■ . .... 7.00 --- — 1............... I ■ । TT’T ■ r " ■ i ■ ‘'1111 " 111 m/z 55.10 83.36% miz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63528: 3-Hexanol 55 59

5000 73 A.... AAAA 31 6.20 6.40 6.60 6.80 7.00

27 m/z 73.05 43.82% 45 84■ i • ■' ■ i ' • • i • ■ ■ • । । । ■ ■ ■ i1 ■ ■ ■ i ■ ■ ■1 i ■ ■ ■ ■ i ■ ■ 4+4 I''1' 121I 1 11 11 ■ ■ ■ ■ i ‘ m/z- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #53531, 3-Hexanol 59 55 6.20 6.40 6.60 6.80 7.00 5000 73 m/z 43.05 32.46% 43 39 69 , ____________ ri r11111111111111" 111 TTT ■' i " ■ ■ i ■ ■ ’' I ■ " ■ i ■ • • I■■111 ■ " 1111" i " • ■ i " miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63527:3-Hexanol 55 6.20 6.40 6.60 6.80 7.00__ m/z 41.10 29.09% 5000 73 31

27

mz-> - - ■ ■ i ■ ■ ■ ■ i'1145 20 25 ' I'111111 30 —4 — d 35 40 45 50 55 84 11 ■ " ' i'1" I' " ' 111 A A 60 65 70 75 80 85 90 6.20 6.40 6.60 6.80 7.00

28168.D NP112701.M Fri Dec 28 09:59:01 2001 Page 4

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