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GCMS analysis results for sample AD28168, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD28168 conducted on January 2, 2002.

NYC-WTC_000034579–000034595

Folder label: “GCMS X 11/23/01 A 12/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2101\28164 .D Vial: 14 Acq On : 22 Dec 2001 5:46 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

6.63 0.42 ng/uL 122847 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexano 102 C6H140 000623-37-0 83 3 3-Hexa: 1 102 C6H140 000623-37-0 83 4 3-He: nol 102 C6H140 000623-37-0 83 Abundance Scan 195 (6.633 min): 28164. D (-) m/z 59.10 100.00% 55 50

5000 73 43 -A....... 39 I 6.20 6.40 6.60 6.80 7.00 ‘11' ■'111'1111''11 ■ ■' । J HHer TTTT 4+ i ■ ■' ■ i ‘ • ■ ■ । ■1 . ।.... ।............ m/z 55.10 85.29% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63527: 3-Hexanol = 59

5000 31 73 4 . ............... 6.20 6.40 6.60 6.80 7.00 m/z 73.0.5 41.02% 27 45 84 I i ‘ I'' ’ ’ I ’ ■ ’' I ■ i ■ ■ ■ ■ i ■1 " 11 " ' l1 IP— > । ■ ■ ■ ■ । ■ >1 111 ■11111 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #53531: 3-Hexanoi 59 55 i ■ ■ ' ■ । ■ ■ ■ ■ । P—.■ 6.20 6.40 6.60 6.80 7.00 5000 73 m/z 43.10 ■ 28.46% 43 39 69 i 111000111‘0uutuutuutnuninneui—uupuuuttuuI;uw—ngur miz— > 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #63528: 3-Hexanol ------------------ 55 59 6.20 6.40 6.60 6.80 7.00 m/z 41.10 23.05% 73 5000

MW 31 27 45 84 " i"11111111 ■ ■ । ■ > ■ ■ । > IPPPT 111 " I " " 111 > i ■ • • ■ i • •1' 11111111 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 6.20 6.40 6.60 6.80 7.00

28164.D NP112701.M Fri Dec 28 09:56:23 2001 Page 3

NYC-WTC_000034589

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NYC-WTC_000034589Source: NYC Law Department, mirrored locally

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