GCMS unknowns analysis results for sample AD27874, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27874.D Vial: 6 Acq On : 20 Dec 2001 8:43 pm Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.69 0.60 ng/uL 522231 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 78 3 3-Hexanol 102 C6H140 000623-37-0 78 4 .3-Hexanol 102 C6H140 __ 000623-37-0 78 Abundance ' Scan 202 (6.694 min): 27874.D (-) m/z 59.10 " 100.00% 55 59 | i 5000 73 43 TTTTPI 39 6.40 6.60 6.80 7.00 ________________ 1 , i, 51 , J_______ 84____________________ TUTT m/z 55.10 81.58% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529: 3-Hexanol 59 55

5000- 31 — ................... 73 27 6.40 6.60 6.80 7.00

44 ! , I m/z 73.05 39.58%

miz-> " I'1" r + i - hT..r ________________ 102 U1 ■" r ■" r " ■ i"111" " I" ■ ■ In ' ■ i ■ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762: 3-Hexanol 59 55 ■ ......... 31 6.40 6.60 6.80 7.00 5000 27 | 43 73 m/ z 3.10 28.91%

________________ 102 mmmmdmmmm 111H■ i■■ ■■ r"■ r1 ‘11""I"" 11 ■" r LAA " r ■" i ■ ’ " i " ■ ■ r ■ ■ ’)' m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531:3-Hexanol " ‘...... “ 59 ____ 6.40 6.60 6.80 Too 55 m/z 41.10 22.47% 5000 73

m/z-> 39 TUIp rr> 111111111111 ■ 11111 43

.। 69 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 AA. 6.40 6.60 6.80 7.00

27874.D NP112701.M Fri Dec 21 09:57:55 2001 Page 2

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