GCMS unknowns analysis results for sample AD27874, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27874.D Vial: 6 Acq On : 20 Dec 2001 8:43 pm Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 2-Hexanol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.80 0.87 ng/uL 763848 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2 -Hexanol 102 C6H140 000626-93-7 83 2 2-Hexanol, (S)- 102 C6H140 052019-78-0 78 3 2-Hexanol, (R) - 102 C6H140 026549-24-6 64 4 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 64 Abundance Scan 214 (6.804 min): 27874.D (-) m/z 45.10 100.00% 45

5000 - ip, n — — । — - 69 ll +mH51 56 , 87 101 miz-?___ 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 111111 ■ I > TTTTTTT ITTTT’T 6.40 rn/z 6.60 69.10 6.80 7.00 7.20 14.53% Abundance #63584:2-Hexanol l 45 %

5000 - P.P 6.40 6.60 6.80 7.00 7.20 69 m/z 41.05 13.12% 19 27 _ ..... thrm 56 87 TWTUUTTTTTTTTT pin TWTTTTTTTTTTTT P I » | H | H I i I i . | i

m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1769: 2-Hexanol, (S) 45 ’I’ ' l • • TTTrr 6.40 6.60 6.80 7.00 7.20 5000 m/ z 43.10 12.14%

19 29 39 69 55 87 TWTTTTTTTTTTTT) TWTOn——p—0T“Bn—]00——0W—T9app m/z—> Abundance 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 45 #1794:2-Hexanol, (R)- 6.40 6.60 AA 6.80 ■rjTi TIT rr 7.00 7.20 m/z 44.10 7.89% 5000

69

m/z-> 9 55 87 TOumupupuup 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 —4 --r TTTTTTNTTTr 6.40 6.60 6.80 7.00 7.20

27874.D NP112701.M Fri Dec 21 09:57:57 2001 Page 3

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