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GCMS analysis results for sample AD27766, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27766 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033343–000033357

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19 01\27766.D Vial: 9 Acq On : 20 Dec 2001 3:13 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T,

6.83 1.41 ng/uL 421510 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 83 2 2 - Hexanol 102 C6H140 000626-93-7 83 3'2- Pentanol , 4-methyl- 102 C6H140 000108-11-2 74 4 2-Kexanol 102 C6H140 000626-93-7 74 Abundance Scan 217 (6.829 min): 27766.D (-) m/z 45.1.0 100.00% 45

5000

41 69 TII _ ) P 6.40 6.60 6.80 7.00 7.20

m/z-> —l .... 5356........ 11 rt . . . > p rrrj , , i , p . > . ( . 10 15 20 25 30 35 40 45 50 55 60 65 70 IPpHp 84 87

75 80 85 90 95 m/ Z 69.10 14.15% Abundance #1792: 2-Hexanol 45

5000- MAIfrA k 6.40 6.60 6.80 7.00 7.20 m/z 41.10 12.99%

J 55 58 69 27,31 3942, ■ I ■ I ■11" 1 > 111 <1 [ ■ ■1 ■ 11 -H+H — 84 87 ■ TTT .. ।. 11. i.. ।.... ।. m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584: 2-Hexanol 45

6.40 6.60 6.80 7.00 7.20 5000- m/z 43.10 10.77%

69 19 27,31 42 ' 56 ! 84 87 —— Tm 1 * | 1 1 ' ' I 1 ‘ ‘ 1 I 1 ‘ ’ 1 I 1 1 1 ’ i ’ • * ‘ I ’ * ’ • TTTT • TT TTIT i P I i i I I i । i p i i i p i m/z-> Abundance 10 15 20 25 30 35 40 45 50 55 60 65 70 #63545: 2-Pentanol, 4-methyl- 45 75 80 85 90 95 NJ TOICITT - 6.40 6.60 6.80 7.00 7.20 m/z 44.10 7.60% 5000-

69 27 39 42 1 I । > : f | i ! I > | > I !T| I I . | I rr> i । i > , iTr TTt 57 TTT .......... ........ 84 87 TWTNDTTTTTTTTTTTTT TIT EAAAAeppy, m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00 7.20

27766.D NP112701.M Thu Dec 20 11:45:26 2001 Page 4

NYC-WTC_000033354

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