GCMS analysis results for sample AD27766, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27766.D Vial: 9 Acq On : 20 Dec 2001 3:13 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.72 1.00 ng/uL 298513 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 90 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H14O _______ 000623-37-0 83 Abundance Scan 205 (6.719 min): 27766.D (-) m/z 59.10 100.00% 55 59

5000 73 43 -A- 39 6.40 6.60 6.80 7.00 r'"r"'i - 51 -rj-r-rt-r ,.. 67 84 +4 TUB00"’CBID1IUMIETTTTr m/ z 55.10 78.70% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance ' ” #63531:3-Hexanol

55 59

5000- 73 — ——————— 6.40 6.60 6.80 7.00 43 m/ z 73.05 43.51% 39 miz-> 20 Ti, H+ I''' " I" 69 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 . " I " TT r ■ ■ ■ i" " r ''' i 11 1 " I

Abundance #1762: 3-Hexanol 59 55 - — । । । i । । ।

31 6.40 6.60 6.80 7.00 5000- 27 43 73 m/z 43 . 10 30.10%

11 102 , 11 -.___________ .________________

A TTTTTT i" " i ■ TT " " i" " r " ■ i " ■ ■ l1"11"111" " I I" " [1 ” 11" " I' m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance ’ #63529: 3-Hexanol । । i • • • • ।

55 59 6.40 6.60 6.80 7.00 m/z 41.10 23.54% 3.1 5000

m/z-> 27

• ■ i ■" • i' TTT 44 " 1111111111 j!! ।! ।11 73

+4 I............ I'1 ______________________ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 102 TITT i ’T’T ri T’TTTITT i > 111111111111111! । _JJ 6.40 6.60 6.80 7.00

27766.D NP112701.M Thu Dec 20 11:45:24 2001 Page 3

NYC-WTC_000033353