GCMS analysis results for sample AD27570, Dec 2001

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Library Search Compound Report

Data File : C : \HPCHEM\1\DATA\DEC1301\27570 . D Vial: 12 Acq On 13 Dec 2001 8:23 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 3-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

10.30 0.60 ng/uL 390187 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 50 2 3-Hexanol 102 C6H140 000623-37-0 50 3 3-Hexanol 102 C6H140 000623-37-0 40 4 3-Hexano1 102 C6H140 000623-37-0 40 Abundance Scan 595 (10.295 min): 27570.D (-) m/z 43.10 100.00% 48 59 55 5000- 73 39 85 Tii T1 T । ! r ' 1 11 1 ' 1 7 '

m/z~> i ■ ■ ■ ■ i l H US + To THPTTTT 100 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 10.00 10.20 10.40 10.60 m/ z 59.10 66.91% Abundance #63527: 3-Hexanol 55 59

5000 73 TIT 31 10.00 10.20 10.40 10.60 m/z 55.10 56.45% 27

m/z-> 20 H 25 30 35 mET 40 45 45 +14 tp...... 1 "I’r i" " i 50 55 60 65 70 75 80 85 84 90 95 100 105 Abundance #63531:3-Hexanol

55 59 ..... A — 10.00 10.20 10.40 10.60 5000 - 73 m/z 57.10 41.24% 1 43 39 69 , Ti, TT‘ । ■ ■ ■ > I ■ ■ ■ ■ । " 11" 11 I' • " i " " i " " i i" " ।" " i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63528: 3-Hexanol ................ /.) .<1111 TT 1 . TIT

55 59 10.00 10.20 10.40 10.60 m/z 41.10 39.88% 5000- 73 A 31

m/z-> m 27 45 TPMDTHTTTTT +44 111111111' 111 T—TT‘ITTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 84 ‘‘‘I ........—4 >44 s 10.00 10.20 10.40 10.60

27570.D NP112701.M Fri Dec 14 12:58:29 2001 Page 2

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