GCMS analysis results for sample AD27769, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC19O1\27769. D Vial: 12 Acq On 20 Dec 2001 5:57 am Operator: GALOS Sample gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 3-Hexanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.72 0.87 ng/uL 261057 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3- Pentanol 88 C5H120 000584-02-1 45 Abundance / Scan 205 (6.722 min): 27769.D (-) m/z 59.10 100.00% 55 59

5000 - 73 43 ------------------ ■ ' I ' ' ' ' I 39 6.40 6.60 6.80 7.00 i1" • r • * • I - T-p-f +44 1............... 1 TTTTTTTTTTTTTIT’’’’ T1 • rrr TT m/z 55.05 79.88% m/z-> 20 25 30 35 40i 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762: 3-Hexanol 59 55 31 5000- TTTTTr TTT 27 43 73 6.40 6.60 6.80 7.00 m/z 73.05 41.51%

miz-> 20 25 i11'' i TT 30 35 40 45 11 4 tmponpr 11111 I 50 55 60 65 70 75 80 ■ I"‘'I“"I 85 102 l ■ ■■ ■ i 90 95 100 105 110 T‘ Abundance #63529: 3-Hexanol

55 59 i ' ■ ■ • i ■ ■ ' ' i 6.40 6.60 6.80 7.00 31 5000 73 m/z 43.10 27.30% 27

44 11 102 T’’’IT’TTT"UT ।| . TTTTTT ri 111 11 i 11 1111 11 ‘ITTTTTTTC’ITTTIT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531: 3-Hexanol 59 6.40 4 - 6.60 6.80 7.00 55 m/ z 41.10 23.00% 5000 73

43

m/z-> | > >H j H i। i ■i.[ 39 Hr +44 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 69+ TT IHnpnl | | | i" ' ■ r 6.40 6.60 6.80 7.00

27769.D NP112701.M Thu Dec 20 11:47:16 2001 Page 3

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