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GCMS analysis results for sample AD27769, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD27769 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033388–000033402

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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Scanned page image, NYC-WTC_000033399
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19 01\27769.D Vial: 12 Acq On : 20 Dec.2001 5:57 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K. L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.83 1.14 ng/uL 340018 1,4-Dichlorobenzene-d4 11.88

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexa nol 102 C6H140 000626-93-7 83 2 2-Hexanol 102 C6H140 000626-93-7 74 3 2-Hexa nol 102 C6H140 000626-93-7 74 4 2-Hexanol, (S) -_________________ 102 C6H140 052019-78-0 64 'Abundance 7 Scan 217 (6.832 min): 27769.D (-) m/ z 45.10 100.00% 45

5000-

। ■ 1 ■ 1 । ' ■ 41 69 6.40 6.60 6.80 7.00 7.20 38 44 TT] 534 84 87 i" • • i ■ ■ m/z 69.10 13.70% m/z-> 1 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584:2-Hexanol ' 45

5000 III ----- 6.40 6.60 6.80 7.00 7.20 m/z 41.10 13.61%

JW 69 84 87 19 2731....... 42. 56 1 1 1 1 1 ' | 1 1 1 ' I1 ' 1 ’ | > rrt | r mi Ur TITTTTT miz--> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63582: 2-Hexanol 45 I

6.40 6.60 6.80 7.00 7.20 5000 m/z .43.10 11.29% 27 69 19 i 31 42, 57 TI't I I I I I I > ( I > I I I I I I I | I I I > pm | , I r 1 84 87 " i" " i1' " i " " 11 " 11'1" 11 m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1792: 2-Hexanol 45 —V 6.40 6.60 6.80 7.00 7.20 m/ z 44 ,05 9.10% 5000- ___

................ I........ .. ...................... 55 58 69 84 87 TTTT — — ‘ i ■ ■ ■111" 11'1 ■ ■ i ■ ■ ■ ■ i'' 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00 7.20

27769.D NP112701.M Thu Dec 20 11:47:18 2001 Page 4

NYC-WTC_000033399

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NYC-WTC_000033399Source: NYC Law Department, mirrored locally

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