GCMS analysis results for sample AD27639, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC18 01\27639.D Vial: 3 Acq On : 18 Dec 2001 5:44 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K . L ********************************************************************* Peak Number 8 3-Hexanol Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

6.69 1.35 ng/uL 310183 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 90 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3 -Hexanol 102 C6H140 000623-37-0 83 Abunda :e Scan 202 (6.693 min): 27639.D (-) m/ z 59.10 100.00% 55 59

5000 73 43 39 6.40 6.60 6.80 7.00

m/z-> -H— + 1PpH Ti 84 i ■ ■ " r ' " I TTTTITTIT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 m/ Z i'" ' i 55.10 82.70% Abundance #63531: 3-Hexanol 59 55

5000- 73 ITTtTTErrf’u— 640 6.60 6.80 7.00 43 m/z 73.05 42.96%

m/z-> 20 25 39 Nil +tTTTTTT —+ 69 , 1' r 1 P ! " I ’ " U ' T‘‘I 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63528:3-Hexanol 59 55 — 6.40 6.60 6.80 7.00 73 5000- m/z 43.10 31.66% 31

27 45 . 11 84 " i" " i" " i H " i " " r " ' i" " i" " i1111 r " 1 r 1111" 11" " I *"' 1 11" 11 r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529:3-Hexanol

55 59 m/z 6.40 6.60 6.80 7.00 24.39% 41.05 -- 5000 31 73

IV/ 27

■' i'1" r mm H 44 102 I TTT’ +4 I..........T > TTTTTTTTTp-TTTTTTTTT.TITTTTTTT WAWV m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00

27639.D NP112701.M Thu Dec 20 11:37:08 2001 Page 8

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