GCMS analysis results for sample AD27765, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19O1\27765 .D Vial: 8 .Acq On : 20 Dec 2001 2:18 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 3-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.68 3.08 ng/uL 692909 1,4-Dichlorobenzene-d4 11.87

Hit# of 5/ Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 90 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 000623-37-0 50 [Abundance /V Scan 201 (6.684 min): 27765.D (-) m/z 59.10 100.00% 55 59

5000 73 43 Tr r । r , 39 6.40 6.60 6.80 7.00

m/z-> 51 TTIH —H ,.. 67 , l""l''' ITT 1T 84 +4 TTTTTT i"" 1 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 101 1’1 U‘ m/z 55.1 0 78.09% 'Abundance #63531: 3-Hexanol

55 59 5000 73 6.40 6.60 6.80 7.00 43 m/z 73.05 42.85% 39 69 . ‘ I 111111" • 'i Tur #44 '' 111 i111' i" " i11' • i1 • • ’ i I“"I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63528:3-Hexanol 59 55 । -.1*1.1 Tn T ' 1 1 TTT . r 1 I < r-l i 6.40 6.60 6.80 7.00 73 5000- m/z 43.10 28.79% 31 27 45 . 11 84 " I" " I" " I'"' I'"' I "'111"' I " " I " " I" " I' I ‘1" I" 1111''' I i' • ’' i ‘'1' i" ' ‘ I r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63527:3-Hexanol IIp r 1 1 55 59 7.00 6.40 6.60 6.80 m/z 41.10 22.90% 5000

m/z-> m 27 31

45 41 tm. + TT 11 ‘ 84 ”I I*1 nT 73

r " 11" " I' 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 JU6.40 6.60 6.80 7.00

27765.D NP112701.M Thu Dec 20 11:23:40 2001 Page 7

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