GCMS analysis results for sample AD27625, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC19O1\27625.D Vial: 15 Acq Oh 20 Dec 2001 10:39 am Operator: GALOS Sample gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K. L ***************************** * * * * ************************************ Peak Number 3 3-Hexanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.72 0.81 ng/uL 234605 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 /Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 000623-37-0 83 Abundance Scan 205 (6.718 min): 27625.D (-) — 59 m/z 59.10 100.00% 55

5000- 73 43 A l ' * ’ ’ I • ‘ 39 6.40 6.60 6.80 7.00 84 m/z-> ‘ T —HHH ‘ItT +44 ITTTT TTTT 1' “ 11 1 r"’i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 i'111 m/ Z 80.65% 'Abundance #63531: 3-Hexanol 59 55

5000 73 =If 6.40 7.00 43 m/z 43.93% 39 TTTTTTTTTTTTTTTT Ip +44 .I ... .... 1''1I TT 11"111TTT ।।।।11 m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762:3-Hexanol 59 55 ----------------- 6.40 6.60 6.80 7.00 31 5000- 27 43 73 m/z 43.10 32.51%

,li . 102 ■ ■ i" ■ ■ i" 1 ■ i ■■ ■ ■ i" '' r " 'i'■' 'i i' “' r " ' i I" " i " " i i"11 TI" m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63527:3-Hexanol A - 59 ob 6.40 6.60 6.80 7.00 m/z 41.10 24.57% 73

JW 5000- 31

m/z-> m 27 'r"'i""I""r' 45 84 +4 I mm TTInuutu"munuEI"TTTT" 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00

27625.D NP112701.M Thu Dec 20 11:40:27 2001 Page 3

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