GCMS analysis results for sample AD27765, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\DEC1901\27765.D Vial: 8 Acq On : 20 Dec 2001 2:18 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 7 3-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.68 3.08 ng/uL 692909 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 90 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 000623-37-0 50 Abundance Scan 201 (6.684 min): 27765.D (-) m/ z 59.10 100.00% 59 55

5000 73 43 Tm—rr 39 6.40 6.60 6.80 7.00 mlz-> " i ‘1 — - 51 TTH ,...... 67 i" "I ""111 + 84 TTTTT 101 r " ' i " " r " ' i ■" ■ i' 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/ z 55.10 78.09% Abundance #63531: 3-Hexanol F9 55

5000- 73 6.40 6.60 6.80 7.00 43 m/z 73.05 42.85% 39 I " " I 69 ! , 11 TITOTTTTTWTTTITTH I' > • • 1111 ‘ I r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63528: 3-Hexanol 59 55 I TIr OInBom 6.40 8.60 6.80 7.00 73 5000 - m/ z 28.79% 31 43.10 27 45 “,‘I‘‘COUETT‘‘OITTTT*TI"T i■"'i"■■r• 84 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63527: 3-Hexanol 55 59 6.40 6.60 6.80 7.00 m/ z 41.10 22.90% 5000 - 73 31

m/z-> m 27 45 TPTTTTTTTTTTTT +4 HH TTTT i1"84 ‘i TT’ITTTT ... | I I n | . 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.40 6.60 6.80 7.00

27765.D NP112701.M Thu Dec.20 11:44:44 2001 Page 7

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