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GCMS analysis results for sample AD27765, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27765 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033311–000033342

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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Scanned page image, NYC-WTC_000033339
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27765.D Vial: 8 .Acq On : 20 Dec 2001 2:18 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 2-Hexanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.79 3.00 ng/uL 673371 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 83 2 2-Hexanol 102 C6H140 000626-93-7 83 3 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 74 4 2-Pentanol, 4-methyl- ________ 102 C6H140 000108-11-2 74 Abundance Scan 213 (6.794 min): 27765.D (-) m/z 45.10 100.00% 45 A

5000- ------------------------- 41 69 6.40 6.60 6.80 7.00 7.20 50 53 56 - *Tuu)mmmupgu| 72 79 84 87 m/z 41.10 14.66% mlz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

J Abundance #1792:2-Hexanol 45

5000- 6.40 6.60 6.80 7.00 7.20 m/z 69.10 13.76% 27,31.... 39 42 1111111'1 "I " 1111111 1 TIIPTTTTnmr 55 58 69 84 87 m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584: 2-Hexanol 45 6.40 6.60 6.80 7.00 7.20 5000 m/ Z 43.10 11.91%

m/z-> Abundance 10 15 19 27,31 42, I । . . .-r-j-r T ri TTT TTTTTTTTTTTT | .... । . . TITT TTTTgm 20 25 30 35 40 45 50 55 60 65 70

45 56

#63546: 2-Pentanol, 4-methyl- 69 111 ■ ■TI 75 ।।।।. 80 84 87 85 90 95 A 6.40 m/ z 6.60 44.10 6.80 7.00 10.90% 7.20

5000-

27 J _ 69 ....15 1920...25 30......... 57 84 87l . . । .-rrrpi I -rp-rrTp-rri-p TIHTTTT TTTurumf m/z-> 10 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00 7.20

27765.D NP112701.M Thu Dec 20 11:44:46 2001 Page 8

NYC-WTC_000033339

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NYC-WTC_000033339Source: NYC Law Department, mirrored locally

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