GCMS analysis results for sample AD28165, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2101\28106.D Vial: 13 Acq On : 22 Dec 2001 4:51 am Operator: GALOS Sample : gems unknown 11/23 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.76 0.59 ng/uL 214380 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol / 102 C6H140 000626-93-7 83 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 74 3 2-Pent nol, 4-methyl- 102 C6H140 000108-11-2 74 4 2-Hexa ol 102 C6H140 000626-93-7 74 Abundance Scan 209 (6.755 min): 28106.D (-) m/z 45.10 100.00% 45

5000

— V 1IP 41 69 6.40 6.60 6.80 7.00 7.20 84 87

miz-> - ....... ........ 472. 10 15 20 25 30 35 40 45 50 55 60 65 70 TTHT mm 75 80 85 90 95 m/z 69.10 14.19% Abundance> #63584:2-Hexanol i 45

5000 —m-pr-r — ------- 6.40 6.60 6.80 7.00 7.20 69 m/ z ,41.10 13.97% 84 87 19 27 31 —44 *TpWHuPTTTTTITTTT OWVutoouuuuuVttTTTTITT ' 56 I mHpT m/z-> Abundance

5000 10 15 20 25 30 35 40 45 50 55 60 65 70 #63546. 2-Pentanol, 4-methyl- 45 75 80 85 90 95

M. m/z .43.10 M+1Ar 7.00 7.20 13.31%

27 ! 69 19 | 31 5742.1 84 87 TTTTTTTTTTTTTTTTTTTT’IT mH.......... 'I" ■rm—p-n rp-n-rpm—r-m-jTi miz- 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63547: 2-Pentanol, 4-methyl- TTTmmTgT 45 6.40 6.60 6.80 7.00 7.20 m/ Z 44.10 10.53% 5000

m/z-> 27

UIuur " i" " r 38,44, tpmHn 10 15 20 25 30 35 40 45 50 55 60 57 69 | 84 87 Tp-r 11WTTTTTTTTTTTTTTTTTTTT 65 70 75 80 85 90 95 A AA -AAAA 6.40 6.60 6.80 7.00 7.20

28106.D NP112701.M Fri Dec 28 09:55:40 2001 Page 3

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