GCMS analysis results for sample AD27628, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19O1\27628 .D Vial: 18 Acq On : 20 Dec 2001 1:24 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 2-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.78 1.23 ng/uL 290261 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 83 2 2-Hexanol 102 C6H140 000626-93-7 83 3 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 78 4 2-Pentanol, 4-methyl-_____________ . 102 C6H140 000108-11-2 74 Abundance Scan 212 (6.785 min): 27628.D (-) m/z 45.10 100.00% 45

5000

41

n/z~> 10 15 20 25 30 35 +40 53 56 69 | 72 1111] ' T rprrTTTTTT]V*Ouu—uTuTTdtmn‘‘‘it 45 50 55 60 65 70 75 80 64 87 85 90 95 6.40 m/Z 6.60 69.10 6.80 7.00 13.46% 7.20

Abundance #63584: 2-Hexanol 45

5000- 114- ■■■ f----------- - 6.40 6.60 6.80 7.00 7.20 69 m/z .41.10 12.90% 56 | 84 87 .......... 41,31..... 44— MW TTTITINIUWTTTTTCPTI m/z—> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1792: 2-Hexanol 45

6.40 6.60 6.80 7.00 7.20 5000- m/ z .43.10 12.53%

27 31 55 58 69 39 42 ( p-rTTp-rTTp-rrrp-rrTp-rrrp-rrTp-rTTp-rrT-p-rT^ 84 87 I " ’' I ""llll'll" Punn m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546: 2-Pentanol, 4-methyl- . T10—————uT 45 6.40 6.60 6.80 7.00 7.20 m/z 44.10 10.18% 5000

27 69 19 31 42 57 Uu—gT TIITTTTI T TITTHTTTTT p-rrnTT-rq-r 84 87 mmmun v AALA Sop 4 044 t 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00 7.20

27628.D NP112701.M Fri Dec 21 09:19:18 2001 Page 6

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