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GCMS analysis results for sample AD27628, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27628 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033159–000033176

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27628.D Vial: 18 Acq On : 20 Dec 2001 1:24 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Hexanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.67 1.10 ng/uL 259498 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 000623-37-0 83 'Abundance . Scan 199 (6.666 min): 27628.D (-) m/ z 59.10 100.00% 55 59 5000- 73 43 39 6.40I 6.60 6.80 7.00 -HHHTTTT 51 +4 HTmt 84 i1"' i ” *' i" " i I |" H | i . r i | . m/ z I55.10 81.34% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531: 3-Hexanol 5(9 55

5000- 73 6.40 6.60 6.80 7.00 43 " 73.OS 44.29% 39 69 TTTTTTTTTTTTTTTT iTtT 44 -TTTTTTTITTT i" " i ‘' r '" i " " i TT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63528: 3-Hexanol 59 55 1 I 1 1 I ' 1 ' ' I I 6.40 I6.60 6.80 7.00 73 5000 m/ z 43 . 10 27.10% 31 27 45 84

NW . 11 ■ i" ■ ■ । pTT [ . . | > 4 i | . I I I ( i" " r • • • r " ’ i • •" i 11 ’' I i " " I" " I" " i" " i' m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529:3-Hexanol ''F ■ ■ TTTPmur 59 6.40 6.60 6.80 7.00 55 m/ z 41.10i 20.54%

-W— 5000 31 73 27

44 mH 44 102 ■ • r ' " r 1If .......... TTIutmEOBHTUTTTTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110

27628.D NP112701.M Fri Dec 21 09:19:16 2001 Page 5

NYC-WTC_000033171

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