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GCMS analysis results, sample AD27626, Jan 2002

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Gas chromatography-mass spectrometry analysis report for sample AD27626 identifying unknown compounds and 2,4-DDD quality control surrogate.

NYC-WTC_000033128–000033142

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27626.D Vial: 16 Acq On : 20 Dec 2001 11:34 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.70 0.82 ng/uL 215120 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 entative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623.-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 000623-37-0 83 Abundance Scan 203 (6.701 min): 27626.D (-) m/z 59.10 100.00% 55 59

5000 73 43 — H-PP---I 39 6.40 6.60 6.80 7.00 i ■ ■ ■ ■ i -HHTT’T 41 IBBIPTU ' I" " i' "' r '" I " " r "' i •" ' i" " i • m/ Z 55.10 35.74% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762:3-Hexanol 59 55 31 —TTPPrrr 5000 27 43 73 6.40 6.60 6.80 7,00 m/z 73.05 44.69% 11 — I ■' " r '" i 102 " I " " I'' " I i ■ ■ ■ ■ i ‘I rf r ■" i m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63527: 3-Hexanol 59 55 I 6.40 6.60 6.80 7.00 5000 73 m/z 43.10 30.09% 31 l 27 45 tilt 84 VI———011TTTTTTTTTTTTTTUTEIITTTTTTTTTETEITTTTTIIEITTT * IVICumu—nuuA"TOO"TTTT m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63528: 3-Hexanol T . । . I | .I 11l 55 59 6.40 6.60 6.80 7.00 m/z 41.10 25.82% 73 5000 __ 31 27 45 l r"■i + +4 HT 84 i" ■ ■ i .p. m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00

27626.D NP112701.M Fri Dec 21 09:17:30 2001 Page 3

NYC-WTC_000033138

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