GCMS analysis results for sample AD27638, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27638.D Vial: 21 Acq On : 20 Dec 2001 4:09 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank '5

R.T. EstConc Area Relative to ISTD R.T.

6.71 0.83 ng/uL 236346 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 90 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 000623-37-0 83 Abundance Scan 203 (6.706 min): 27638.D (-) m/z 59.10 100.00% 59 55

5000 73

39 43 -4 . .. 6.40 6.60 6.80 7.00

m/z--> mH If’ a 1WPPP7 I ‘" I" •' I ‘ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 m/z TT TTTTT TTT 55.10 79.84% Abundance #63531: 3-Hexanol 59 55

5000 - 73 . ................... 6.40 6.60 6.80 7.00 43 m/z 73.05 44.05% 39 ' 1 | " 11111 । । । •« • • । T +TT I" ' ‘ I " " i •1 TT +69 1111 111 । r. । 11«11 m 11 । 11 । । । V m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63528: 3-Hexanol 55 59। 1 I I | I I ! 1

6.40 6.60 6.80 7.00 73 5000- m/z 43.10 31.46% 31

27 45 . 11 84 WIITITTCTTTTTTTTTTTTT TTTTTTTT0I00UTIITTTTT m/z->20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529:3-Hexanol *t11/T*—/TTELTET/-ET11/T/IT

55 59 6.40 6.60 6.80 7.00 m/z 41.10 23.74%

_NW_ 31 5000- 73 27

44 " i" " i1 TTT HH +4 — । । < . m । rn । (। । 111 । < n । I ’" ’ I r 102 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00

27638 .D NP112701 .M Fri Dec 21 09:21:05 2001 Page 3

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