GCMS analysis results for sample AD27276, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27276.D Vial: 4 Acq On : 19 Dec 2001 8:56 am Operator: GALOS Sample . : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 3-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

10.28 1.57 ng/uL 379027 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 43 2 3-Hexanol 102 C6H140 000623-37-0 38 3 3-Hexanol 102 C6H140 000623-37-0 37 4 3-Hexanol 102 C6H140 000623-37-0 37 Abundance Scan 593 (10.277 min): 27276.D (-) m/z 43.10 100.00% 4 55 59 5000- 73 85 m - —Z — . 39 10.00 10.20 10.40 10.60

miz-> ‘‘i - 4 Tp —l 89 T TTTTT T‘ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 100 m/ z 59.10 55.97% (Abundance #63527:3-Hexanol 55 59

5000- 73 —------ — i ■ ■ 31 10.00 10.20 10.40 10.60 m/ z 55.10 50.65% 27 45 84 m/z-> T i" "I TTT trnrrTn-rryr TT 44 I 1 1' ' I I •1' • I ’ “ ' i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 'Abundance #1762: 3-Hexanol

31 55 59 A10.00 10.20 10.40 10.60 5000- 27 | 43 73 m/ z 41.10 36.23%

111 1 * 1 " I ’1 " I " H P b t t| TTETTTTT Ji TTTT 102 FTTTTTETTTTTTTTT’TTTT’T’TIIT I ’1111 i‘ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529:3-Hexanol ---------------- -P . . 55 59 10.00 10.20 10.40 10.60 m/ z 57.1.0 34.60% 5000 31 73 27

44 " I" ■' I' TTT —H +44 jmpoe TT I.. 11 f. 11TTTTTTTTT ... I102 .... I... TTT A ---------------- TEIIF m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 10.00 10.20 10.40 10.60

27276.D NP112701.M Thu Dec 20 11:38:36 2001 Page 4

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