GCMS analysis results for sample AD27678, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\2 7678 . D Vial: 5 Acq On : 19 Dec 2001 10:48 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 3-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

10.28 1.38 ng/uL 333860 1,4-Dichlorobenzene-d4 11.85

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 47 2 3-Hexanol 102 C6H140 000623-37-0 40 3 3-Hexanol 102 C6H140 000623-37-0 38 4 3-Hexanol 102 C6H140 000623-37-0 28 Abundance' Scan 593 (10.277 min): 27678.D (-) m/z 43.10 100.00% 43 59 55 5000 73 ----- 39 85 10.00 10.20 10.40 10.60

m/z-> U 4 +51+ mmH Ur TTT i ” " i " ■' i 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 m/ z 100 59.10 61.05% Abundance #63527: 3-Hexanol 59 55

5000- 31 73 1 1'I 10.00 10.20 10.40 10.60 m/z 55.10 52.71% 27 45 84 i'1 ■' i TTTTTT +44 tm 1T '' I V m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762: 3-Hexanol 59 55 A10.00 10.20 10.40 10.60 31 5000 27 43 73 m/ z 41.10 37.18%

. 102 T" " I ' • ‘ • I i) i11111 TTEJi’ITTTTTTTTTT ITTETTTTIIETTTIE’TTT I'" ’ I T‘ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529:3-Hexanol ................. - $===

55 59 m/ z 10.00 10.20 10.40 10.60 57.10 35.66% 31 5000 73 27

m/z-> " I ■ " ' I' 44 rr mH 44 tpm TTTTTIPTIIITTTTTTT 102 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 .............. — —AA 10.00 10.20 10.40 10.60

27678.D NP112701.M Thu Dec 20 11:41:14 2001 Page 5

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