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GCMS analysis results for sample AD27954, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS analysis of sample AD27954 conducted on January 2, 2002.

NYC-WTC_000034097–000034110

Folder label: “GCMS X 11/20/01 A 12/20/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27954.D Vial: 10 Acq On : 21 Dec 2001 12:22 am Operator: GALOS Sample : gems unknown 11/20 Inst. : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.70 0.52 ng/uL 169892 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 000623-37-0 83 Abundance Scan 203 (6.701 min): 27954.D (-) m/z 59.10 100.00% 55 59

5000 73 I 43 ■ ■ । ■ 11 ’ ’ ' ■ i 11 11 i

miz-> i" " l mP He 39 1 + 11——— m/z 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 55.10 6.80 7.00 83.51% Abundance #63528: 3-Hexanol 55 T 59

5000 73 • I o. A LA,.... 31 6.40 6.60 6.80 7.00 27 m/z 73.05 42.25% .... i........ 45 ,il .______ , 84 ___________ ‘ ‘ l " ‘ ‘ i ‘1'' I ‘‘ i' ‘" I " '1 i " '' i " " 111 I' " 1 r '1' I “ " 111" 11 ^T111' F'111" " 111111" " 11 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531; 3-Hexano! 50 55 7 6.40 6.60 6.80 7.00 5000 73 m/z 43..10 31.50% 43 39 1 .!. 69 j p...।.i।।j,...11j।■H 11 ■ 11 ITT' 111 >■ 1111111111> 11 m 1111111 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529: 3-Hexanol -r-T-1 -,-T-rr-)

| 59 6.40 6.60 6.80 7.00 1 55 m/z 41.10 23.89% 31

JU 5000 73 27 44 . .... . .... Ji ,.... , . .......... 102... " I ’ " ' I' " I " ' I' ’ " I'1'11'' ■' I " 11 H H I T’Tr 11111111 H 11 1111 , i n j 11111111 111 n 11, i i 1111 n 11 m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00____

27954.D NP112701.M Fri Dec 21 09:59:19 2001 Page 3

NYC-WTC_000034107

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NYC-WTC_000034107Source: NYC Law Department, mirrored locally

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