GCMS unknowns analysis results for sample AD27873, Jan 2002

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Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD27873 conducted on January 2, 2002.

NYC-WTC_000034032–000034045

Folder label: “GCMS X 11/20/01 A 12/20/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27873.D Vial: 5 Acq On : 20 Dec 2001 7:48 pm Operator: GALOS Sample : gems unknown 11/20 Inst. : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.70 0.53 ng/uL 213910 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H14O 000623-37-0 83 3 3-Hexanol 102 C6H14O 000623-37-0 83 4 3-Hexanol 102 C6H140 000623-37-0 83 Abundance Scan 203 (6.703 min): 27873.D (-) m/z 59.10 100.00% 55 59

5000 73

39 43 6.40 -A \...................... ' 1 I 1 ' * ' I ' ‘ ' • I 6.60 6.80 7.00 i ■ ■" i" " i ■1" I —•i•h 41 tpmT • | |■■.<| HIjH..|...>। .i|.... ।. m/z 55.10 82.75% miz- 20 25 30 35 40 45 505560 65 70 75 80 85 90 95 100 105 110 Abundance #63528:3-Hexanol 55 59

73 4 . । TInT TIT ′ > r i । i i i i । 5000 31 6.40 6.60 6.80 7.00 27 m/z 73.05 41.59%

m/z-> m .. 4.. 44 I....... M 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 84_________________ 11 U .. 1 K| I I 111 11 I I | I I I I | I

Abundance #33531: 3-Hexanol 59 55 • • । \___________ • i ■ > • ' I * ' ’ ' I ’ ‘ ‘ • I 6.40 '6.60 6.80 7.00 5000 73 m/z 4 3.10 30.91% 43 39 ....... 69 m/z-> Abundance TTYiTT-rpT-rrp-rrTTTi-rrp-rrriTTTTp-rTTp-^^ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #1762:3-Hexanol 59 11।1111111111111111111111111111

6.40 A.... 6.60 6.80 7.00 55 m/z 41.10 20.42% 31 5000

_ A__ 27 43 73

___________________ 102 miz "T1 ‘ T “'I" tmr "O—UT0—TTOT“‘I"TT"TTTTOOTr 20 25. 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00

27873.D NP112701.M Fri Dec 21 09:57:25 2001 Page 3

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GCMS unknowns analysis results for sample AD27872, Jan 2002 · Box DEP Box 22

NYC-WTC_000034018

Laboratory report documenting GCMS analysis for unknown compounds and surrogate recovery in sample AD27872 conducted on January 2, 2002.

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