GCMS analysis results for sample AD27956, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19 01\27956.D Vial: 12 Acq On : 21 Dec 2001 2:12 am Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.69 0.51 ng/uL 163861 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 3 -Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 _______ 000623-37-0 83 Abundance Scan 202 (6.693 min): 27956.D (-) m/z 59.10 100.00%| 55 59 5000 73 43 rr 1 1 • • > । । । I | । I i • j i i • i

6.40 6.60 6.80 7.00 mmmmm HP 4# TTT TJTTTTpTrrpTTTTTTTTyTTTTp-^^ , T‘ m/z 55.10 84.17 miz-? 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529: 3-Hexanol ... TT 59 55

31 5000 73 —IA 1-P 27 6.40 6.60 6.80 7.00 m/ z 73.0.5 41.10 ______________ 102 .............."I mpH ■ T‘I1‘ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #93527; 3-Hexano! . 59 55 ________ ._______ ' ' i ' ' ■ ' i ■ ■ ■ • i ■ ■ • ■ i • ’ 6.40 6.60 6.80 7.00 5000 73 m/z 3.05 29.88 31

27 i 45 . J | 84 TTTTTTTTT .।....।.,,,।.।>111, ।.... |,,,. 1111111 i 11111 TI"I0uuOTT miz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63528: 3-Hexanol 55 59। 6.40 6.60 6.80 7.00 m/z 41.05 24.33? 5000

miz-> 27 .... .... 31

45 mTTTTT +4 t ‘ITTITTT 84 73

TIIUITUTT’TI . T-rp-rrqT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 W 6.40 6.60 6.80 7.00

27956.D NP112701.M Fri Dec 21 10:00:35 2001 Page 3

NYC-WTC_000034134