GCMS analysis results for sample AD27624, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27624.D Vial: 13 Acq On : 20 Dec 2001 6 :52 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.72 0.90 ng/uL 278959 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexano 102 C6H140 000623-37-0 83 2 3-Hexa: 1 102 C6H140 000623-37-0 83 ol 3 3-Hexa-- 102 C6H140 000623-37-0 83 4 3-Hexanol Abundance f 102 C6H140 000623-37-0 83 Scan 205 (6.724 min): 27624.D (-) m/z 59.10 100.00% 55 59

5000 - 73 43 - TIom ■ ■ । ■ ■ > • । 39 6.40 6.60 6.80 7.00 miz-> TTTTTTTTTTT . .HHHH T-p-r 41 IPPTTTH 1T 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 r•”i i'" ’ r " * i TT m/ z 55.10 76.00% Abundance ................ .......... #63529: 3-Hexanol 59 55

5000 31 =PImTrrrrur 73 27 6.40 6.60 6.80 7.00 m/z 73.05 38.93% 44 I " '' I +4 I........... TTTT’TTTTTTTTTT — T^'T 102 m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63527: 3-Hexanol 59 55 6.40 6.60 6.80 7.00 5000- 73 m/z ). 10 28.66% 31

27 | 45 84 -rp-rrT-pT-TT-j-. | JI | "’’’I’TTII’TOIIIT TTTTTTTTTTTTTTTTJTTTTTTTTTTTTTT^^ 111' ‘1' 111'11' m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #63528:3-Hexanol —! j A V • ■ i ‘ ■ i

55 59 6.40 6.60 6.80 7.00 m/z 41.05 22.35%

JW 73 5000 31

27 45 " r' • • i • ‘ T ....... . I ■' ■ 11 ■ ■ ' 'T'-'' +4 IP TH TTTTTICTTTIITT 84 miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00

27624.D NP112701.M Thu Dec 20 11:39:48 2001 Page 3

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