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GCMS analysis results for sample AD27985, Jan 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD27985 conducted on January 2, 2002, noting unknown compounds and surrogate recovery.

NYC-WTC_000034457–000034471

Folder label: “GCMS X 11/21/01 A 12/21/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19O1\27985.D Vial: 26 Acq On : 21 Dec 2001 6:45 am Operator: GALOS Sample : gems unknown 11/21 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.69 0.41 ng/uL 131254 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 .Tentative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 83 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol Abundance Scan 201 (6.687 min): 27985.D (-) 102 C6H140 000623-37-0 83 m/ z 59.10 100.00% 55 59

5000 73 i । । । । । _A L . — — 43 6.40 6.60 6.80 7.00 TrpTrrrp-rrrj-r mmm 4+ ................ ' r ■ " i" ■ ■ i" " i" " r " i ■ ■111 ‘ ■1 ■ r m/z 55.10 86.18% rn/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63528: 3-Hexanol 55 59

5000- 31 73 -4 .......... 6.40 6.60 6.80 7.00 m/z 73.05 47.19% 27 45 84_________________ m/z-> i' •" ir" ' i + — ' i" " ।" r " ■ i " " i" " i" " i" " i' 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63527; 3-Hexanol 00 59 . _________ 6.40 6.60 6.80 7.00 5000 73 .05 28.23% 31

27 • 45 84 .................I' r "' i ■ r“ ■i T l”"ll i ■ •" r " ■ i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762:3-Hexanol TT-r 59 6.40 6.60 6.80 7.00 55 m/z 41.10 24.43% 31

_ MW , ,_ 5000 27 43 73

" i ■ • ■ ■ i' ’ T TITT ’1"1111"011101101—Cu102 TTH ______________________ —C—T37T miz-> 20 25 30 35 40 45 50 55 60 65 70.75 80 85 90 95 100 105 110 6.40 6.60 6.80 7.00

27985.D NP112701.M Fri Dec 28 09:30:58 2001 Page 3

NYC-WTC_000034467

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NYC-WTC_000034467Source: NYC Law Department, mirrored locally

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