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GCMS analysis results for sample AD27956, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report detailing GCMS analysis of sample AD27956 conducted on January 2, 2002.

NYC-WTC_000034124–000034137

Folder label: “GCMS X 11/20/01 A 12/20/01

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\DEC 1901\27956.D Vial: 12 Acq On : 21 Dec 2001 2:12 am Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.80 0.74 ng/uL 238647 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H140 000626-93-7 83 2 2-Pentanol, 4-methyl- 102 C6H140 000108-11-2 83 3 2 -Pentanol, 4-methyl- 102 C6H140 000108-11-2 83 4 2-Hexanol, (R) -_________ _____ 102 C6H140 _______ 026549-24-6 78 Abundance Scan 214 (6.803 min): 27956.D (-) m/z 45.10 100.00% 45

5000 TTmnnnn Tu

miz-> m 41 56 69 84 87 < ■■ ■ I ■ ■ ■■ 11<..।.111..11..r11" " 11u f।' I' 11"11111 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 m/z 41.10 ' ' I ' ' ' ' I ' ' 7.00 13.86% 7.20

Abundance!

5000 #63584:2-Hexanol 45

69 JUA 6.40 m/z 6 60 43.05 6.80 4M5APAf 7.00 7.20 12.44% | , mlz-> 19 27,31 lyn ‘ I . UUIIUTTTOTTTTO—TTT 10 15 20 25 30 —4+ 35 40 45 50 tTTTTT I WII—56*—0*1mWTNNIPTTTT 84 87 55 60 65 70 75 80 85 90 95 {Abundance - #83547; 2-Pentanol, 4-methyl .................................................. 45

6.40 6.60 6.80 7.00 7.20 5000 m/z 69.1.0 12.34% 27 69 38 45 : 57 i 84 87 •p-m-p-TT.-p ITT pTTTTTTTTp-TTTTTT Hr ■ | | | | i > I r. ■ i | ■ > r> | ■ I I I | I I I I | I I I I p I miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1773: 2-Pentanol, 4-methyl- -I ' ' ' ■ I ■ ' ' ■ I ' • 45 6.40 6.60 6.80 7.00 7.20 m/z 44.1.0 9.13% 5000

69 27 mT — rm-p- ' > > 111111 >1" I <1 '| i 42 57 84 87 "i" " i" ■1 r 1111"" 11' 1AAA/ 44 44 miz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00 7.20

27956.D NP112701.M Fri Dec 21 10:00:37 2001 Page 4

NYC-WTC_000034135

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NYC-WTC_000034135Source: NYC Law Department, mirrored locally

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