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GCMS analysis results for sample AD27545, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD27545 for unknown compounds and surrogates on December 18, 2001.

NYC-WTC_000033433–000033447

Folder label: “GCMS X 11/15/01 A 12/13/01

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Scanned page image, NYC-WTC_000033443
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1301\27545 .D Vial: 4 Acq On 13 Dec 2001 1:07 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

6.81 0.47 ng/uL 191991 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 /Tentative ID MW MolForm CAS# Qual

1 2-Hexanol/ 102 C6H140 000626-93-7 83 2 2-Hexanol 102 C6H140 000626-93-7 78 3 2 -Pentanol , 4-methyl- 102 C6H140 000108-11-2 74 4 2-Pentanol, Abundance / 4-methyl- ___________ Scan 214 (6.808 min): 27545.D (-) 102 C6H140 000108-11-2 74 m/ z 45.10 100.00% 45

5000- Tmrmud— 69 6.40 6.60 6.80 7.00 7.20 87 56 207 r " ■ r ■" i • TpH TT TH r" t m/ z 69.10 14.98% m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200 210 Abundance #63584: 2-Hexanol 45

............ _ 5000- 6.40 6.60 6.80 7.00 7.20 m/ z 41.05 -------- 14.81%

A 69 56 27 87 . ........TTTTIEI 11111 TT,............. - I" 111 ’ITT li I" " I' • ” I I • •' • I' ’ •' 11'" I" " I m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 Abundance #1792: 2-Hexanol 45 --- 6.40 6.60 6.80 7.00 7.20 5000- m/ z .43.10 12.71%

27 1 55 69 87 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 Abundance #63547: 2-Pentanol, 4-methyl- II TTTTTTTTrrru 45 6.40 6.60 6.60 7.00 7.20 m/z 44.05 8.52% 5000-

27 57 62 87 TTP # I I TTTTTTTTTTTTTTTT I I I I | I I I I | M M | I I I I | I I I I | I I I I | I III TTTTTTTTTTTTTTT I I I | • t I « | I » ■ I | ADAA “d ABs m/z-> 10 20 3C 4G 50 60 7C 80 90 100110120130140,150160170180190 200 210 6.40 6.60 6.80 7.00 7.20

27545.D NP112701.M Fri Dec 14 12:54:32 2001 Page 3

NYC-WTC_000033443

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NYC-WTC_000033443Source: NYC Law Department, mirrored locally

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