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GCMS analysis results for sample AD27545, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD27545 for unknown compounds and surrogates on December 18, 2001.

NYC-WTC_000033433–000033447

Folder label: “GCMS X 11/15/01 A 12/13/01

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Scanned page image, NYC-WTC_000033442
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1301\27545.D Vial: 4 Acq On 13 Dec 2001 1:07 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.56 0.80 ng/uL 325629 1,4-Dichlorobenzene-d4 11.86

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 91 3 2-Hexanone 100 C6H120 000591-78-6 91 4 2-Hexanone 100 C6H120 000591-78-6 90 Abundance Scan 187 (6.560 min): 27545.D (-) m/ z 43.10 100.00% 43 58 5000

39 53. | . 71 85 100 6.20 TIT TIPTT P TII TI - 1IMHT P , 1 ,, T TIM TT ' i " " I m/z 58.10 54.07% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556:2-Hexanone 43

58 r — _I_I_P_ / T I N_r_P_J_I_- I 5000- 6.20 6.40 6.60 6.80 7.00 m/z 57 05 16.26% 27 100 i1'111 39 71 85 TMMTH T—IBpuna’ir 11PMPNITTTTT m/z—>20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m Abundance 43 #63385:2-Hexanone

6.20 6.40 V 6.60 6.80 14.30% 7.00 5000- 58 m/z 41.05 _..

LMW 29 | 39 71 8.5 100 1* ] m q in) U’EIITT’TII TTT 'i 1I‘ l. ' I'." I' ■ "I " " I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63386:2-Hexanone ' ' I 1 1 ' ' i ' ' ' ■ I 1 1 1 1 1 1 1 ’ - 43 6.20 6.40 6.60 6.80 7.00 m/z 100.05 8.80% 5000 58 29 71 100 85 A.. — — "111111' TTPTTT IBuur m ——B‘0"1TTh!_ _I______ _____ —TEI‘II‘T m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80 7.00

27545.D NP112701.M Fri Dec 14 12:54:30 2001 Page 2

NYC-WTC_000033442

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NYC-WTC_000033442Source: NYC Law Department, mirrored locally

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