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GCMS analysis results for sample AD27764, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27764 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033285–000033310

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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Scanned page image, NYC-WTC_000033301
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27764.D Vial: 7 Acq On : 19 Dec 2001 12:38 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration ParamS: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 8 2-Hexanone Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

6.56 1.23 ng/uL 310468 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 91 2 2-Hexanone 100 C6H120 000591-78-6 91 3 2-Hexanone 100 C6H120 000591-78-6 91 4 2-Hexanone 100 C6H120 000591-78-6 90 'Abundance ' Scan 188 (6.563 min): 27764.D (-) m/z 43.10 100.00% 43 58 5000-

71 85 100 6.20 6.4C 6.60 6.80 7.00

miz-> 34l + 53 | . — — m 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/z 58.10 54.47% Abundance #63385: 2-Hexanone 43

5000 58 Pr --------------------- 6.20 40 6.60 6.80 7.00 29 n/z. 41.10 16.55% 39 71 85 100 m/z—> m I T +1WP12)—mmPTTTPTTTTTTTTTT TTTTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63384: 2-Hexanone 43 6.20 AAAAA 6.40 6.60 6.80 7.00 5000 58 m/z 57.. 10 15.65% 29 I 39 | I 71 100 ’ 85 m P AW >' i >>" i p-rrrp-rr r " ' i " " I " " I " " 11" 111" 11111' i1' m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63386:2-Hexanone ■ ' I ' ' 'll11 » I I ' ' 43 6.20 6.40 6.60 6.80 7.00 m/z 100 . 05 8.37%

5000- 58 29 100 111111111 TPP >>i'i'l 'I............ । *1111 ■ 111 > 71 ।! ■ ■ • । 85 •i ■ ■••I■ ■ • ■ । ।• i •" ' i m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80 7.00

27764.D NP112701.M Thu Dec 20 11:43:34 2001 Page 8

NYC-WTC_000033301

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NYC-WTC_000033301Source: NYC Law Department, mirrored locally

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