GCMS analysis results for sample AD27764, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27764.D Vial: 7 Acq On : 19 Dec 2001 12:38 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 3-Hexanone Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

6.46 0.99 ng/uL 250445 1,4-Dichlorobenzene-d4 11.85

Hit# of 5 entative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3 -Hexanone 100 C6H120 0005,89-38-8 90 3 3-Hexanone 100 C6H120 000589-38-8 64 4 3-H anone 100 C6H120 000589-38-8 53 Abundance Scan 177 (6.462 min): 27764.D (-) m/z 43.10 100.00% 100.000 i 43 57 !

MW I 71 5000 100 —ITCCECLmLL-r11111118T 6.201 6.40 6.60 6.80 85 ............... H 111"111" " i H1 TTTTT TTTTT r m/z !57.10 98.55% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358:3-Hexanone 43 57

5000 71 100 A 6.20 6.40 W 6.60 6.80 m/z 71.05 57.38% 85 -PPP m4 +T ■ i "'' i r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 57 . ---------------- 6.20 6.40 6.60 6.80 29 71 m/z 100.15 30.05% 5000 I

100 85 ■11" ■ ■ i" " i" " i " ■ ■ i i ■' " i •' ■' r " ' i' " ' i 'r"'r'"i TTTTIu) miz-> 20 25 30 35 4 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357:3-Hexanone 43 6.20 6.40 6.60 6.80

1 57 41.10 29.21% 29

5000 71

100

m/z-> Tp mm TTTTTTTTTTT 85 TTTTT’TT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 r 6.20 AAAAA 6.40 6.60 6.80

27764.D NP112701.M Thu Dec 20 11:43:32 2001 Page 7

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