GCMS analysis results for sample AD27622, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27622.D Vial: 22 Acq On : 20 Dec 2001 5:04 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.57 2.39 ng/uL 687152 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanon 100 C6H120 000591-78-6 91 2 2-Hexan e 100 C6H120 000591-78-6 91 3 2-Hexa one 100 C6H120 000591-78-6 91 4 2-Hi anone 100 C6H120 000591-78-6 91 [Abundance Scan 189 (6.572 min): 27622.D (-) m/z 43.10 100.00% 43

58 5000

53 | , --- IINT 87 71 -mmmmmm m/ z 85 100 A 6.20 6.40 6.60 6.80 7.00 58.10 54.03% miz-?20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63385:2-Hexanone 43

5000 58 ,2 6.20 6.40 6.60 6.80 7.00 29 m/ z 41.05 15.69% ! 71 85 100 " r " ' i " TTT TTTTTTTTT i ■ ■ ■11 ■ • " I ■'' ■ i T‘ m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556: 2-Hexanone 43

6.20 58 5000 m/ z 57.. 10 15.04%

27 85 100

miz- Abundance ' ■ •■ i ■ • • ■ i ■ 71 ‘1‘111012111811101" ‘‘I"t111"S1-1‘1"II"T"IIITTTTTE"II"t ‘iI n*1 * । • - "I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105

43 #63386: 2-Hexanone T-rm-p

6.20 P0.m V. 6.40 6.60 m/Z 10 0 . 05 6.80 8.99% 7.00

5000 58 29 100

m/z-> " r '' ■ i' -H i‘ mTPF71 ■ r' " r 85 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 I" " I 11 “'11' 6.20 6.40 6.60 6.80 7.00

27622.D NP112701.M Fri Dec 21 09:16:43 2001 Page 2

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