GCMS analysis results for sample AD27622, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27622.D Vial: 22 Acq On : 20 Dec 2001 5:04 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.71 0.89 ng/uL 255157 1,4-Dichlorobenzene-d4 11.86

Hit# Of 5 entative ID MW MolForm CAS# Qual

1 3-Hexanol 102 C6H140 000623-37-0 90 2 3-Hexanol 102 C6H140 000623-37-0 83 3 3-Hexanol 102 C6H140 000623-37-0 83 4 3-Hexanol 102 C6H140 000623-37-0 83 Abundance Scan 204 (6.710 min): 27622.D (-) m/z 59.10 100.00% 55 59

5000- 73 43 A X r --- 39 6.40 6.60 6.80 7.00 । । । । PPP m - ■ i ■ ■ — . . .... ,.69, i11111111111 ' i ' ' ' ' i ■ ■ ■ ■ i ' ' ‘ ■ i ' ■ m/z 55.10 84.94% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 'Abundance #63531: 3-Hexanol 59 55

5000 73 6.40 6.60 A 6.80 1 ' i ' ' 1 ’ I 7.00 43 m/ Z 45.84% 73.05 ■ i ■ ■ • ■ i • ■ •' i ■ ■ ■ ■ । 39 ■ 11 ■' 1 i' ■ ■ ■ i' ■ 4 --69 i ■ • ■ ■ । ■ ■' ■ । ■1 11 ' ■ ■ ' i ‘ ' i ■ ■'' i ■

mlz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 [Abundance #63528: 3-Hexanol 59 55 1

6.40 6.60 6.80 7.00 73 5000 - m/z 43.10 30.88% 31

27 45 .11 . : 84 ■ i ■ ■ ■ ■ i ■ ■ ■ ‘ i ■ • । ■ ■ ■ ■ । ■ i ■ • • • i • • • ■ l >■

AA > ■ i ■. • > i. • ■ ■ । ■ ■ ■ i • ■ ■ ■ i • • ■ ■ । ■ i ■ >

m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 ^Abundance #63527: 3-Hexanol — $ 6.40 6.60 6.80 7.00 55 m/z 41.10 24.79% 5000 73 31

27 11 J 1 11 111'111'1' I TP ++ 1 T 1111111 45 84 m/z-> 11201" 1 — 25 30 35 40 45 50 55 60 65 70 75 ■ 1 * i * > ■ ■ i ■ ■ ' * i • < । ■ i >

80 85 90 6.40 6.60 6.80 TP01 7.00

27622.D NP112701.M Fri Dec 21 09:16:47 2001 Page 3

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