GCMS analysis results for sample AD27769, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC19O1\27769. D Vial: 12 Acq On : 20 Dec 2001 5:57 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.48 0.76 ng/uL 225835 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 . Tentative ID MW MolForm CAS# Qual

1 3-Hexan e 100 C6H120 000589-38-8 91 2 3-Hex. one 100 C6H120 000589-38-8 91 3 3-He: none 100 C6H120 000589-38-8 78 4 3-H anone 100 C6H120 000589-38-8 64 Abundance. Scan 179 (6.483 min): 27769.D (-) m/ z 43.10 100.00% / 43 57 71 5000 — 100 6.20 6.40 6.60 6.80

miz-> 34 ......H H 85 TTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 p m/z »■ i ............... 1'1111 57.10 93.43% Abundance #63358:3-Hexanone 43 57

5000 71 PPP ■ • i • r 6.20 6.40 6.60 6.80 100 m/ z 71.05 53.55% 85 11'111 I • ’" I — +t i" i r ■ ■' i' ■'' I " ■ i ■ ■' ■ I P m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance

5000- 43

29 #1528: 3-Hexanone 57 1

71 ----- 6.20 6.40 6.60 m/z 100.15 A— 6.80 30.57% 100 85 i‘ 'I I'''' I''' • I I' " ' I Tn i ■'' ■ r '■' i" " i'1" I''1' I" ' ■ I P m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 - Abundance #63356: 3-Hexanone \.... — 29 43 57 6.20 6.40 6.60 6.80 m/ z 41.10 26.90%

. W 5000 71

100

m/z-> " i" " i1 20 25 —38,4 ■1............ I' 30 35 40 45 50 55 r " ' i" " i 60 65 70 + 85—BIIUITTT TCUI 75 80 85 90 95 100 105 P 6.20 6.40 6.60 6.80

27769.D NP112701.M Thu Dec 20 11:47:12 2001 Page 1

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